Analysis of Pesticides in Food and Environmental Samples
Published 7 February 2008
Citations178
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Abstract
Analysis of pesticides in food and environmental samples , Analysis of pesticides in food and environmental samples , کتابخانه دیجیتال جندی شاپور اهواز
Keywords
ChemistryAgricultural and Biological Sciences
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Journal of Chromatography ATrace analysis of pesticides by gas chromatography
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Journal of Chromatography ASolid-phase micro-extraction–gas chromatography–(tandem) mass spectrometry as a tool for pesticide residue analysis in water samples at high sensitivity and selectivity with confirmation capabilities
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The combination of selective extraction by SPME and highly selective determination by GC-MS-MS made possible ultra-selective and essentially error-free determination of pesticides in complex environmental samples.
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Journal of Chromatography AExtraction methodology and chromatography for the determination of residual pesticides in water
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Critical Reviews in Food Science and NutritionCurrent Trends in Immunoassay-Based Kits for Pesticide Analysis
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Journal of Chromatography AApplicability of headspace solid-phase microextraction to the determination of multi-class pesticides in waters
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The applicability of headspace solid-phase microextraction (HS-SPME) to pesticide determination in water samples was demonstrated by evaluating the effects of temperature on the extraction of the pesticides.
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Capillary electrophoresis-mass spectrometry with an electrospray ionization interface was applied for the quantitative analysis of imazamox pesticide in well water, potable water, and pond water and the detector response was linear over the concentration range of 50-1 ng/ml.
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For most of the 13 pesticides tested, there were no differences in recovery between in-house extracted disks and shipped disks, indicating the suitability of disks to concentrate and transport pesticides extracted from water samples.
Journal of AOAC InternationalStability of Pesticides on Solid-Phase Extraction Disks After Incubation at Various Temperatures and for Various Time Intervals: Interlaboratory Study
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Pesticide-specific losses occurred on the C18 disks in this study, underlining the importance of temperature and time interval when water is extracted at remote field locations and the SPE disks containing the extracted pesticides are transported or shipped to a laboratory for elution and analysis.
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